真人平台

国产保健食品备案凭证(千雌愫牌锌维生素B6 泛酸咀嚼片)

真人平台  fabushijian: 2019-11-25 09:53:12  

 

chanpinmingcheng

qiancisupaixinweishengsub6 fansuanjujiaopian

beianren

shanxidetongbaoyiyaokejiyouxiangongsi

beianrendizhi

shanxishengxianshigaoxinquxinxinggongyeyuanchuangyedadao22haobangonglou3lou301shi

beianjielun

anzhao《zhonghuarenmingongheguoshipinanquanfa》《baojianshipinzhuceyubeianguanlibanfa》dengfalv、guizhangdeguiding,yuyibeian。

beianhao

真人平台shijianbeig202061001897

fujian

1 chanpinshuomingshu;2 chanpinjishuyaoqiu

beizhu

2020nian11yue03ri

fujian1

baojianshipinchanpinshuomingshu

shijianbeig202061001897

───────────────────────────────────────────

qiancisupaixinweishengsub6 fansuanjujiaopian

【yuanliao】rusuanxin,yansuanbiduochun,d-fansuangai

【fuliao】zhetang,d-ganlutangchun,maiyahujing,rutang,ningmengsuan

真人平台【gongxiaochengfenjihanliang】meipianhan: xin 6mg weishengsub6 2mg fansuan 3.5mg

【shiyirenqun】xuyaobuchongxin、weishengsub6 、fansuande chengren

【bushiyirenqun】17suiyixiarenqunjiyunfu、rumu

真人平台【baojiangongneng】buchongxin、weishengsub6、fansuan

【shiyongliangjishiyongfangfa】meiri 1 ci, meici 2 pian,shiyongfangfa: jujiaoshiyong

【guige】1.0 g/pian

【zhuzangfangfa】mifeng,yinliangganzaochubaocun

【baozhiqi】24geyue

真人平台【zhuyishixiang】benpinbunengdaitiyaowu。shiyirenqunwaiderenqunbutuijianshiyongbenchanpin。buyichaoguotuijianlianghuoyutongleiyingyangsutongshishiyong

fujian2

baojianshipinchanpinjishuyaoqiu

真人平台shijianbeig202061001897

真人平台───────────────────────────────────────────

真人平台qiancisupaixinweishengsub6 fansuanjujiaopian

【yuanliao】rusuanxin,yansuanbiduochun,d-fansuangai

【fuliao】zhetang,d-ganlutangchun,maiyahujing,rutang,ningmengsuan

【shengchangongyi】benpinjingganzao(50℃)dengzhuyaogongyijiagongzhicheng。

真人平台【zhijiejiechuchanpinbaozhuangcailiaodezhonglei、mingchengjibiaozhun】

gutiyaoyonggaomidujuyixipingyingfuhe《koufugutiyaoyonggaomidujuyixiping》(ybb 00122002);suliaofangdaopinggaiyingfuhe《baozhuangrongqi suliaofangdaopinggai》(gb/t 17876)。

真人平台【ganguanyaoqiu】yingfuhebiao1deguiding。

biao 1 ganguanyaoqiu

xiang  mu

zhi  biao

se ze

baise

ziwei、qiwei

weitianweisuan、wuyiwei

zhuang tai

wuzhengchangshilikejianwailaizazhi

【jianbie】

wu

真人平台【lihuazhibiao】yingfuhebiao2deguiding。

biao2 lihuazhibiao

xiang  mu

zhi  biao

jiancefangfa

qian(yi pbji),mg/kg

≤2.0

gb 5009.12

zongshen(yi asji),mg/kg

≤1.0

gb 5009.11

真人平台zonggong(yi hgji),mg/kg

≤0.3

gb 5009.17

huifen,%

≤9

gb 5009.4

真人平台1 qiandeceding yiju《gb 5009.12》

1.1 yiqi

1.1.1 yuanzixishouguangpuyi: peishimoluyuanzihuaqi,fuqiankongxinyinjideng

1.1.2 fenxitianping

真人平台1.1.3 kediaoshidianrelu

1.2 shiji

1.2.1 xiaosuan(hno3)。

1.2.2 gaolvsuan(hclo4)

1.2.3 linsuanerqingan(nh4h2po4)

真人平台1.2.4 xiaosuanba(pd(no3)2)

1.2.5 biaozhunpinlaiyuanchundu: guojiayousejinshujidianzicailiaofenxiceshizhongxin,chundu: 1000 μg/ml。

1.3 yiqitiaojian;

bozhang283.3nm;xiafeng0.5nm;dengdianliu8~12mv;ganzao: 85℃~120℃/40s~50s;huihua: 750℃/20s~30s;yuanzihua: 2300℃/4s~5s。

真人平台1.4 biaozhunpinrongyezhibei:

真人平台1.4.1 qianbiaozhunzhongjianye(1.00mg/l): zhunquexiquqianbiaozhunrongye(1000mg/l)1.00mlyu1000mlrongliangpingzhong,jiaxiaosuanrongye(5+95)zhikedu。

真人平台1.4.2 qianbiaozhunxilierongye: fenbiexiquqianbiaozhunzhongjianye(1.00mg/l)0ml、0.500ml、1.00ml、2.00ml、3.00ml、4.00mlyu100mlrongliangpingzhong,jiaxiaosuanrongye(5+95)zhikedu,hunyun。ciqianbiaozhunxilierongyedenongdufenbieweiqian0µg/l、5µg/l、10µg/l、20µg/l、30µg/l、40µg/l。

1.5 yangpinrongyezhibei: chengqugutishiyang1gyuzhuixingpingzhong,jia10mlxiaosuan、0.5mlgaolvsuan,zaikediaoshidianrelushangxiaojie。ruoxiaohuayechengzonghese,zaijiaxiaosuan,xiaojiezhimaobaiyan,xiaohuayechengwusetouminghuolvedaihuangse。quchuzhuixingping,lengquehouyongshuizhuanyizhi10mlrongliangpingzhong,hunyunbeiyong。tongshizuoshijikongbaishiyan

1.6 ceding: anzhiliangnongduyoudidaogaodeshunxufenbiejiang10μlqianbiaozhunxilierongyehe5μllinsuanerqingan-xiaosuanbarongyetongshizhurushimolu,yuanzihuahouceqixiguangduzhi,yubiaozhunxiliebijiaodingliang。

1.7 jieguojisuan

(ρ-ρ0)×v

真人平台x = ——————————

m×1000

shizhong:

x—yangpinzhongqiandehanliang,mg/100g;

真人平台a—yangpinzhong×××defengmianji;

真人平台ρ—biaozhunrongyezhongqiandezhiliangnongdu,μg/l;

ρ0—biaozhunrongyezhong×××××biaozhunpindefengmianji;

m—yangpinzhiliang,g;

真人平台v—shiyangxiaohuayededingrongtiji,ml。

1000--huansuanxishu

2 shendeceding yiju《gb 5009.11》

2.1 yiqi

真人平台2.1.1 yuanziyingguangguangpuyi

2.1.2 fenxitianping

2.1.3 kediaoshidianrelu

2.2 shiji

2.2.1 qingyanghuana(naoh)

真人平台2.2.2 qingyanghuajia(koh)

真人平台2.2.3 pengqinghuajia(kbh4):fenxichun

2.2.4 liuniao(ch4n2o2s):fenxichun

2.2.5 yansuan(hcl)

2.2.6 xiaosuan(hno3)

2.2.7 liusuan(h2so4)

真人平台2.2.8 gaolvsuan(hclo4)

2.2.9 xiaosuanmei([mg(no3)2·6h2o]): fenxichun

2.2.10 yanghuamei(mgo): fenxichun

2.2.11 kanghuaixuesuan(c6h8o6)

2.2.12 biaozhunpinlaiyuanchundu: guojiayousejinshujidianzicailiaofenxiceshizhongxin,chundu: 1000 μg/ml。

2.3seputiaojian

fugaoya: 260v;shenkongxinyinjidengdianliu: 50ma~80ma: zaiqi: yaqi;zaiqiliusu: 500ml/min;pingbiqiliusu: 800ml/min;celiangfangshi: yingguangqiangdu;dushufangshi: fengmianji。

2.4biaozhunpinrongyezhibei:

2.4.1shenbiaozhunzhongjianye(1.00mg/l): zhunquexiqushenbiaozhunrongye(1000mg/l)1.00mlyu1000mlrongliangpingzhong,jiaxiaosuanrongye(2+98)zhikedu。

2.4.2shenbiaozhunxilierongye: qu25mlrongliangping6zhi,yicizhunquejiarushenbiaozhunzhongjianye(1.00mg/l)0ml、0.10ml、0.25ml、0.50ml、1.50ml、3.00ml(fenbiexiangdangyushennongdu0.0ng/ml、4.0ng/ml、10ng/ml、20ng/ml、60ng/ml、120ng/ml),gejialiusuanrongye(1+9)12.5ml,liuniao+kanghuaixuesuanrongye2ml,bujiashuizhikedu,hunyunhoufangzhi30minhouceding。

2.5 yangpinrongyezhibei: qugongshipincufenlg ,zhi50mlganguozhong,tongshizuoliangfenshijikongbai。jiaxiaosuan20ml,gaolvsuan4ml,liusuan1.25ml,fangzhiguoye。cirizhiyudianrebanshangjiarexiaojie。jixujiarezhixiaojiewanquan,zaichixuzhengfagaolvsuandebaiyansanjin,liusuandebaiyankaishimaochu。lengquejiashui25ml,zaizhengfazhiliusuanmaobaiyan。lengque,yongshuijiangneirongwuzhuanru25mlrongliangpingzhong,jiaruliuniao+kanghuaixuesuanrongye2ml,bujiashuizhikedu。antongfazuokongbaishiyan。

真人平台2.6ceding: jiangshijikongbai、biaozhunxilierongyeyiciyinruyiqijinxingyuanziyingguangqiangdudeceding。yiyuanziyingguangqiangduweizongzuobiao,shennongduweihengzuobiaohuizhibiaozhunquxian,dedaohuiguifangcheng。xiangtongtiaojianxia,jiangyangpinrongyefenbieyinruyiqijinxingceding。genjuhuiguifangchengjisuanchuyangpinzhongshenyuansudenongdu,jide。

2.7 jieguojisuan

(c-c0)×v×1000

x = ———————————————

真人平台m×1000×1000

shizhong:

x—yangpinzhongshendehanliang,mg/100g;

真人平台c—shiyangbeiceyezhongshendecedingnongdu,ng/ml;

真人平台c0 —shiyangkongbaixiaohuayezhongshendecedingnongdu,ng/ml;

真人平台v —shiyangxiaohuayezongtiji,ml;

m —yangpinzhiliang,g;

1000--huansuanxishu。

3 gongdeceding yiju《gb 5009.17》

3.1 yiqi

真人平台3.1.1 yuanziyingguangguangpuyi

3.1.2 fenxitianping

3.2 shiji

真人平台3.2.1xiaosuan(hno3)

真人平台3.2.2liusuan(h2so4)

3.2.3zhonggesuanjia(k2cro7)

3.2.4biaozhunpinlaiyuanchundu: guojiayousejinshujidianzicailiaofenxiceshizhongxin,chundu: 1000 μg/ml。

3.3 seputiaojian

guangdianbeizengguanfugaoya: 240v,gongkongxinyinjidengdianliu: 30ma,yuanzihuaqiwendu: 300℃;zaiqiliusu: 500ml/min;pingbiqiliusu: 1000ml/min。

真人平台3.4 biaozhunpinrongyezhibei:

3.4.1gongbiaozhunzhongjianye(10μg/ml): xiqu1.00mlgongbiaozhunrongye(1.00mg/ml)yu100mlrongliangpingzhong,yongzhonggesuanjiadexiaosuanrongye(0.5g/l)xishizhikedu,hunyun,cirongyedenongduwei10μg/ml,yu4℃bingxiangzhongbiguangbaocun。

3.4.2gongbiaozhunshiyongye(50ng/ml): xiqu0.5mldegongbiaozhunzhongjianye(10μg/ml)yu100mlrongliangpingzhong,yongzhonggesuanjiadexiaosuanrongye(0.5g/l)xishizhikedu,hunyun,cirongyedenongduwei50ng/ml,xianyongxianpei

真人平台3.4.3fenbiexiqu50ng/mlgongbiaozhunshiyongye0.00ml、0.20ml、0.50ml、1.00ml、1.50ml、2.00ml、2.50mlyu50mlrongliangpingzhong,yongxiaosuanrongye(1+9)xishizhikedu,yaoyun,gezixiangdangyugongnongduwei0.00ng/ml、0.20ng/ml、0.50ng/ml、1.00ng/ml、1.50ng/ml、2.00ng/ml、2.50ng/ml。

真人平台3.5yangpinrongyezhibei: qugongshipinxifenlg ,zhixiaohuazhuangzhizhuixingpingzhong,jiabolizhushuli,jia45mlxiaosuanhe10mlliusuan,zhuandongzhuixingpingfangzhijubutanhua。zhuangshanglengningguanhou,xiaohuojiare,daikaishifapaotingzhijiare,fapaotingzhihou,jiarehuiliu2xiaoshi。xiaojiedaoyangpinwanquanrongjie,chengwuse,fanglenghouconglengningguanshangduanxiaoxinjia20mlshui,jixujiarehuiliu10fenzhongfangleng,yongshiliangshuichongxilengningguan,chongxiyebingruxiaohuayezhong,jiangxiaohuayejingbolimianguolvyu100mlrongliangpingzhong,yongshaoliangshuixidizhuixingping、lvqi,xidiyebingrurongliangpingnei,jiashuizhikedu,hunyun。tongfazhibeishijikongbairongye。

3.6ceding: shezhihaoyiqizuijiatiaojian,lianxuyongxiaosuanrongye(1+9)jinyang,daidushuwendinghou,zhuanrubiaozhunxilieceliang,huizhibiaozhunquxian。zhuanrushiyangceliang,xianyongxiaosuanrongye(1+9)jinyang,shidushujibenhuiling,zaifenbiecedingshiyangkongbaiheshiyangxiaohuaye,meicebutongshiyangqiandouyingqingxijinyangqi。shiyangcedingjieguoanshi(1)jisuan。

3.7 jieguojisuan

(c-c0)×v×1000

x = ———————————————

真人平台m×1000×1000

shizhong:

真人平台x—yangpinzhonggongdehanliang,mg/100g;

真人平台c—shiyangbeiceyezhonggongdecedingnongdu,ng/ml;

c0 —shiyangkongbaixiaohuayezhonggongdecedingnongdu,ng/ml;

v —shiyangxiaohuayedingrongzongtiji,ml;

m—yangpinzhiliang,g;

真人平台1000--huansuanxishu。

4 huifendeceding an《gb 5009.04》ceding

4.1 yiqi

4.1.1 mafulu;

4.1.2 fenxitianping;

真人平台4.1.3 shiyingganguohuociganguo;

真人平台4.1.4 ganzaoqi(neiyouganzaoji);

4.1.5 dianreban

4.2ganguoyuchuli

qudaxiaoshiyideshiyingganguohuociganguozhigaowenluzhong,zai550℃±25℃xiazhuoshao30min,lengquezhi200℃zuoyou,quchu,fangruganzaoqizhonglengque30min,zhunquechengliang。zhongfuzhuoshaozhiqianhouliangcichengliangxiangchabuchaoguo0.5mgweihengzhong。

4.3chengyang: zhunquechengquyangpin3g,jingquezhi0.0001g,jiangyangpinjunyunfenbuzaiganguonei,buyaoyajin。

真人平台4.4yangpinchuli: gutishiyangxianzaidianrebanshangxiaohuojiareshishiyangchongfentanhuazhiwuyan,ranhouzhiyugaowenluzhong,zai550℃±25℃xiazhuoshao4h,lengquezhi200℃zuoyou,quchu,fangruganzaoqizhonglengque30min,zhunquechengliang。zhongfuzhuoshaozhiqianhouliangcichengliangxiangchabuchaoguo0.5mgweihengzhong。

真人平台4.5shiyangzhonghuifendehanliang

m1 - m2

x= —————————— ×100

m3 - m2

shizhong:

x—yangpinzhonghuifendehanliang,danweiweikemeibaike(g/100g);

真人平台m1—ganguohehuifendezhiliang,danweiweike(g);

真人平台m2 —ganguodezhiliang,danweiweike(g);

真人平台m3—ganguoheshiyangdezhiliang,danweiweike(g);

真人平台100--danweihuansuanxishu

真人平台【weishengwuzhibiao】yingfuhebiao3deguiding。

biao3 weishengwuzhibiao

xiang  mu

zhi  biao

jiancefangfa

junluozongshu,cfu/g

≤20000

gb 4789.2

dachangjunqun,mpn/g

≤0.92

gb 4789.3 mpn jishufa

meijunhejiaomu,cfu/g

≤50

gb 4789.15

jinhuangseputaoqiujun

≤0/25g

gb 4789.10

shamenshijun

≤0/25g

gb 4789.4

【gongxiaochengfenhuobiaozhixingchengfenzhibiao】yingfuhebiao4deguiding。

biao4 gongxiaochengfenzhibiao

xiang  mu

zhi  biao

jiancefangfa

真人平台meipianhan xin(yiznji)

4.5-7.5 mg

gb/t5009.14

meipianhan weishengsub6 (yibiduochunji)

1.6-3.6 mg

gb/t 5009.197

meipianhan fansuan(yifansuanji)

2.8-6.3 mg

gb/t 5009.210

真人平台1xin(zn)hanliangjiance: yiju《gb 5009.14》

1.1yuanli: shiyangjingxiaojiechulihou,jinghuoyanyuanzihua,zai213.9nmchucedingxiguangdu。zaiyidingnongdufanweineixindexiguangduzhiyuxinhanliangchengzhengbi,yubiaozhunxiliebijiaodingliang。

1.2 shiji

1.2.1xiaosuan(hno3)

1.2.2gaolvsuan(hclo4 )

真人平台1.2.3biaozhunpinlaiyuanchundu: guojiayousejinshujidianzicailiaoyanjiuzhongxin,chundu: 1000 μg/ml

1.3yiqi

1.3.1yuanzixishouguangpuyi: peihuoyanyuanzihuaqi,xinkongxinyinjideng。

1.3.2fenxitianping: ganliang0.1mghe1mg。

1.3.3kediaoshidianrelu

1.4 biaozhunquxiandezhibei:

真人平台1.4.1xinbiaozhunzhongjianye(100mg/l): zhunquexiquxinbiaozhunrongye(1000mg/l)10mlyu100mlrongliangpingzhong,jiaxiaosuanrongye(5+95)zhikedu,hunyun。

真人平台1.4.2xinbiaozhunxilierongye: fenbiexiquxinbiaozhunzhongjianye(100μg/ml)0ml,1.00ml,2.00ml,4.00ml,8.00ml,10mlyu100mlrongliangpingzhong,jiaxiaosuanrongye(5+95)dingrongzhikedu,hunyun。zhichengxinzhiliangnongduwei0 μg/ml、1.00 μg/ml、2.00 μg/ml、4.00 μg/ml、8.00 μg/ml、10.00 μg/mldebiaozhunxilierongye。

1.5yangpinchuli

qubenpinxifen0.5g,zhi150mlzhuixingpingzhong,jia10mlxiaosuan、0.5mlgaolvsuan,zaikediaoshidianrelushangxiaojie。ruoxiaohuayechengzonghese,zaijiaxiaosuan,xiaojiezhimaobaiyan,xiaohuayechenghuangsetouming。quchuzhuixingping,lengquehouyongshuizhuanyizhi1000mlrongliangpingzhong,yongshaoliangshuixidi2~3ci,hebingxidiyeyurongliangpingzhongbingyongshuidingrongzhikedu,hunyunbeiyong。tongshizuoshijikongbaishiyan。

真人平台1.6yangpinceding: jiangxinbiaozhunxilierongyeannongduyoudidaogaodeshunxudaoruhuoyanyuanzihuaqi,zai213.9nmdebozhangchucedingxiguangdu,yixindezhiliangnongduweihengzuobiao,xiangyingdexiguangduzhiweizongzuobiao,zhizuobiaozhunquxian。tongfacedingkongbairongyeheshiyangdaiceyedexiguangduzhi,yubiaozhunxiliebijiaodingliang。

1.7jieguojisuan

真人平台(ρ-ρ0)×v×s×1000

x = ——————————

m×1000×1000

shizhong:

x—yangpinzhongxindehanliang,mg/pian;

ρ—yangpincedingyezhongxindezhiliangnongdu,μg/ml;

ρ0 —yangpinkongbaiyezhongxindezhiliangnongdu,μg/ml;

m—yangpinzhiliang,danweiweig;

真人平台v—shiyangxiaohuayedingrongtiji,ml;

s—pingjunpianzhong,danweiweig;

1000—danweihuansuanxishu。

2weishengsub6hanliangjiance: yiju《gb/t 5009.197》

2.1yuanli: jiangfensuihunyundepianjishiyongjiachun+shui+linsuan=100+400+0.5jinxingtiquhexishi,genjugaoxiaoyexiangsepuziwaijianceqiwaibiaofadingxingdingliangjiance。。

2.2shiji

真人平台2.2.1jiachun: youjichun。

2.2.2yijing: sepuchun。

2.2.3linsuan: fenxichun。

真人平台2.2.4 1-guiwanhuangsuanna: gaoxiaoyexiangsepuyongshiji。

2.2.5biaozhunpinlaiyuanchundu: zhongjianyuan,chundu99.9%

2.3yiqi

2.3.1gaoxiaoyexiangsepuyi: daiziwaijianceqi。

2.3.2fenxitianping: ganliang0.1mg。

2.3.3chaoshengboqingxiqi。

1.3.4lixinji。

2.4seputiaojian

a)sepuzhu: c18(zhuzhang150mm,neijing4.6mm,lijing5 μm)

b)zhuwen: shiwen。

c)liudongxiang: 1-guiwanhuangsuannarongye(1.22g→850ml)+yijing+linsuan=850+150+1。

d)liusu: 1.0 ml/min

真人平台e)ziwaijiancebozhang: 280m

真人平台f)jinyangliang: 10μl

真人平台2.5 biaozhunquxiandezhibei:

真人平台2.5.1yansuanbiduochunbiaozhunchubeiye(1.000mg/ml): zhunquechengliangyikouchushuifendeyansuanbiduochunbiaozhunpin0.0500g,rongyushuibingdingrongzhi50ml。

2.5.2yansuanbiduochunbiaozhunshiyongye(0.25mg/ml): zhunquexiquyansuanbiduochunbiaozhunchubeiye5 ml,jiajiachun+shui+linsuan=100+400+0.5hunherongyedingrongzhi20ml。

2.6yangpinchuli

qubenpinyanxihunyun,chengquxifen2g(jingquedao0.001g),jiarujiachun+shui+linsuan=100+400+0.5hunherongye50ml,shinongduweimeihaoshengzhonghanyansuanbiduochun0.25mg。chaoshengtiqu5minhouyi3000 r/minlixin5min,shangqingyejing0.45μmweikonglvmoguolvhoudaijinyang。

2.7yangpinceding: jiangyansuanbiduochunbiaozhunshiyongyeheshiyangrongyeyicizhuruyexiangsepuyi,jilusepufengmianji,yongwaibiaofajisuanchushiyangcedingyezhongyansuanbiduochundenongdu。

2.8jieguojisuan

真人平台h1×c×v×s× 1000

x = ——————————

h2×m×1000

shizhong:

x—yangpinzhongyansuanbiduochundehanliang,danweiweihaokemeipian(mg/pian);

h1—shiyangfengmianji;

真人平台c—biaozhunrongyenongdu,danweiweihaokemeihaosheng(mg/ml);

v—dingrongtiji,danweiweihaosheng(ml);

真人平台h2—biaozhunrongyefengmianji;

s—pingjunpianzhong,danweiweike(g);

m—shiyangdechengyangliang,danweiweike(g);

1000—danweihuansuanxishu。

3fansuanhanliangjiance yiju《gb 5009.210》

真人平台3.1 yuanli: shiyangzhongdekanghuaixuesuanyongpianlinsuanrongjiechaoshengtiquhou,yiliziduishijiweiliudongxiang,jingfanxiangsepuzhufenli,yongpeiyouziwaijianceqideyexiangsepuyijiance。yisepufengbaoliushijiandingxing,waibiaofadingliang。

3.2 shiji

3.2.1pianlinsuan(hpo3)n: hanliang(yihpo3ji)≥38%。

3.2.2linsuanerqingjia(kh2po4)

3.2.3shiliuwanjisanjiajixiuhuaan(c19h42brn): sepuchun

真人平台3.2.4jiachun(ch3oh): sepuchun

3.2.5biaozhunpinlaiyuanchundu: zhongjianyuan,chundu: 96.8%。

3.3 yiqi

3.3.1gaoxiaoyexiangsepuyi: peiyouziwaijianceqi。

真人平台3.3.2 phji: jingdu±0.01。

真人平台3.3.3 fenxitianping: ganliangwei0.1g、1mg、0.01mg。

真人平台3.3.4 chaoshengboqingxiqi

3.3.5 lixinji: zhuansu≥4000 r/min。

3.4 seputiaojian

真人平台a)sepuzhu: c18(zhuzhang250mm,neijing4.6mm,lijing5 μm)

b)zhuwen: 25℃

真人平台c)liudongxiang: a: 6.8glinsuanerqingjiahe0.91gshiliuwanjisanjiajixiuhuaan,yongshuirongjiebingdingrongzhi1l(yonglinsuandiaophzhi2.5~2.8);b;100%jiachun。ana: b=98: 2hunhe,guo0.45μmlvmo,chaoshengtuoqi。

d)liusu: 0.7ml/min

e)ziwaijiancebozhang: 245nm

真人平台f)jinyangliang: 20μl

真人平台3.5 biaozhunquxiandezhibei:

3.5.1 l(+)kanghuaixuesuanbiaozhunchubeirongye(1.000mg/ml): zhunquechengqubiaozhunpinl(+)kanghuaixuesuan0.01g(jingquezhi0.01mg),yong20g/ldepianlinsuanrongyedingrongzhi10ml。

真人平台3.5.2 l(+)kanghuaixuesuanbiaozhunxiliegongzuorongye: fenbiezhunquexiqul(+)kanghuaixuesuanbiaozhunrongyezhongjianye0.ml,0.05ml,0.50ml,1.0ml,2.5ml,5.0ml,yong20g/ldepianlinsuanrongyedingrongzhi100ml。biaozhunxiliegongzuorongyedefenbienongduwei0 μg/ml、0.5 μg/ml、5.0 μg/ml、10.0 μg/ml、25.00 μg/ml、50.0 μg/ml。

3.6 yangpinchuli

qubenpinshiliang,yanxi,jingmichengding0.5g(jingquezhi0.001g),yong20g/ldepianlinsuanrongyejiangshiyangzhuanyizhi50mlrongliangpingzhong。zhenyaorongjiebingdingrong。yaoyun,quanbuzhuanyizhi50mllixinguanzhong,chaoshengtiqu5fenzhonghou,yu4000 r/minlixin5min,qushangqingyeguo0.45μmshuixianglvmo,zuoweigongshipinrongye。

3.7 yangpinceding: fenbiexiqul(+)kanghuaixuesuanbiaozhunxiliegongzuorongye10μlzhurugaoxiaoyexiangsepuyizhong,cedingxiangyingdefengmianji,yifengmianjiweizongzuobiao,yibiaozhuncedingyenongduweihengzuobiaohuizhibiaozhunquxian,jisuanhuiguifangcheng。gongshipinjinggaoxiaoyexiangsepuyifenxi,cedefengmianji,caiyongwaibiaofatongguoshangshubiaozhunquxianjisuanqinongdu。

3.8jieguojisuan

ρ×v×s× 1000

x = ——————————

真人平台m×1000×1000

shizhong:

x —yangpinzhongkanghuaixuesuandehanliang,danweiweihaokemeipian(mg/pian);

ρ—congbiaozhunquxianshangchadedekanghuaixuesuandenongdu,danweiweiweikemeihaosheng(μg/ml);

v—dingrongtiji,danweiweihaosheng(ml);

真人平台s—pingjunpianzhong,danweiweike(g);

真人平台m—shiyangdechengyangliang,danweiweike(g);

1000—danweihuansuanxishu。

【zhongliangchayizhibiao】

yingfuhe《zhonghuarenmingongheguoyaodian》zhong“zhijitongze”xiangxiapianjideguiding。

【yuanfuliaozhiliangyaoqiu】

1、rusuanxin: yingfuhegb 1903.11 《shipinanquanguojiabiaozhun shipinyingyangqianghuaji rusuanxin》deguiding

2、yansuanbiduochun: yingfuhegb 14753 《shipinanquanguojiabiaozhun shipintianjiaji weishengsub6(yansuanbiduochun)》deguiding

真人平台3、d-fansuangai: yingfuhe《zhonghuarenmingongheguoyaodian》zhongfansuangaideguiding

4、zhetang: yingfuhexianxing《zhonghuarenmingongheguoyaodian》deguiding

5、d-ganlutangchun: yingfuhegb 1886.177 《shipinanquanguojiabiaozhun shipintianjiaji d-ganlutangchun》deguiding

真人平台6、maiyahujing: yingfuhegb/t 20884 《maiyahujing》deguiding

7、rutang: yingfuhegb25595 《shipinanquanguojiabiaozhun rutang 》deguiding

8、ningmengsuan: yingfuhegb 1886.235 《shipinanquanguojiabiaozhun shipintianjiaji ningmengsuan》deguiding




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