真人平台

chanpinmingcheng	真人平台qiancisupaixinyansuanweishengsucjujiaopian
beianren	shanxidetongbaoyiyaokejiyouxiangongsi
beianrendizhi	真人平台shanxishengxianshigaoxinquxinxinggongyeyuanchuangyedadao22haobangonglou3lou301shi
beianjielun	anzhao《zhonghuarenmingongheguoshipinanquanfa》《baojianshipinzhuceyubeianguanlibanfa》dengfalv、guizhangdeguiding，yuyibeian。
beianhao	shijianbeig202061001898
fujian	1 chanpinshuomingshu；2 chanpinjishuyaoqiu
beizhu

真人平台2020nian11yue03ri

fujian1

baojianshipinchanpinshuomingshu

shijianbeig202061001898

───────────────────────────────────────────

真人平台qiancisupaixinyansuanweishengsucjujiaopian

真人平台【yuanliao】rusuanxin,yanxianan,l-kanghuaixuesuan

【fuliao】zhetang,d-ganlutangchun,maiyahujing,rutang

【gongxiaochengfenjihanliang】meipianhan: xin 6mg yanxianan 9mg weishengsuc 35mg

【shiyirenqun】xuyaobuchongxin、yanxianan、weishengsucde chengren

真人平台【bushiyirenqun】17suiyixiarenqunjiyunfu、rumu

真人平台【baojiangongneng】buchongxin、yansuan、weishengsuc

真人平台【shiyongliangjishiyongfangfa】meiri 1 ci， meici 2 pian，shiyongfangfa: jujiaoshiyong

【guige】1.0 g/pian

真人平台【zhuzangfangfa】mifeng，yinliangganzaochubaocun

【baozhiqi】24geyue

【zhuyishixiang】benpinbunengdaitiyaowu。shiyirenqunwaiderenqunbutuijianshiyongbenchanpin。buyichaoguotuijianlianghuoyutongleiyingyangsutongshishiyong

fujian2

baojianshipinchanpinjishuyaoqiu

shijianbeig202061001898

真人平台───────────────────────────────────────────

真人平台qiancisupaixinyansuanweishengsucjujiaopian

真人平台【yuanliao】rusuanxin,yanxianan,l-kanghuaixuesuan

【fuliao】zhetang,d-ganlutangchun,maiyahujing,rutang

真人平台【shengchangongyi】benpinjingganzao（50℃）dengzhuyaogongyijiagongzhicheng。

真人平台【zhijiejiechuchanpinbaozhuangcailiaodezhonglei、mingchengjibiaozhun】

真人平台gutiyaoyonggaomidujuyixipingyingfuhe《koufugutiyaoyonggaomidujuyixiping》（ybb 00122002）；suliaofangdaopinggaiyingfuhe《baozhuangrongqi suliaofangdaopinggai》（gb/t 17876）。

真人平台【ganguanyaoqiu】yingfuhebiao1deguiding。

biao 1 ganguanyaoqiu

xiang  mu	zhi  biao
se ze	rubaisezhibaise
ziwei、qiwei	weisuanweitian、wuyiwei
zhuang tai	wuzhengchangshilikejianwailaizazhi

【jianbie】

wu

【lihuazhibiao】yingfuhebiao2deguiding。

biao2 lihuazhibiao

xiang  mu	zhi  biao	jiancefangfa
qian（yi pbji），mg/kg	≤2.0	gb 5009.12
zongshen（yi asji），mg/kg	≤1.0	gb 5009.11
zonggong（yi hgji），mg/kg	≤0.3	gb 5009.17
huifen，%	≤9	gb 5009.4

1 qiandeceding yiju《gb 5009.12》

1.1 yiqi

真人平台1.1.1 yuanzixishouguangpuyi: peishimoluyuanzihuaqi，fuqiankongxinyinjideng

1.1.2 fenxitianping

1.1.3 kediaoshidianrelu

1.2 shiji

真人平台1.2.1 xiaosuan（hno3）。

1.2.2 gaolvsuan（hclo4）

真人平台1.2.3 linsuanerqingan（nh4h2po4）

1.2.4 xiaosuanba（pd（no3)2）

真人平台1.2.5 biaozhunpinlaiyuanchundu: guojiayousejinshujidianzicailiaofenxiceshizhongxin，chundu: 1000 μg/ml。

1.3 yiqitiaojian;

真人平台bozhang283.3nm；xiafeng0.5nm；dengdianliu8~12mv；

ganzao: 85℃~120℃/40s~50s；huihua: 750℃/20s~30s；yuanzihua: 2300℃/4s~5s。

真人平台1.4 biaozhunpinrongyezhibei:

真人平台1.4.1 qianbiaozhunzhongjianye（1.00mg/l）: zhunquexiquqianbiaozhunrongye（1000mg/l）1.00mlyu1000mlrongliangpingzhong，jiaxiaosuanrongye（5+95）zhikedu。

1.4.2 qianbiaozhunxilierongye: fenbiexiquqianbiaozhunzhongjianye（1.00mg/l）0ml、0.500ml、1.00ml、2.00ml、3.00ml、4.00mlyu100mlrongliangpingzhong，jiaxiaosuanrongye（5+95）zhikedu，hunyun。ciqianbiaozhunxilierongyedenongdufenbieweiqian0µg/l、5µg/l、10µg/l、20µg/l、30µg/l、40µg/l。

1.5 yangpinrongyezhibei: chengqugutishiyang1gyuzhuixingpingzhong，jia10mlxiaosuan、0.5mlgaolvsuan，zaikediaoshidianrelushangxiaojie。ruoxiaohuayechengzonghese，zaijiaxiaosuan，xiaojiezhimaobaiyan，xiaohuayechengwusetouminghuolvedaihuangse。quchuzhuixingping，lengquehouyongshuizhuanyizhi10mlrongliangpingzhong，hunyunbeiyong。tongshizuoshijikongbaishiyan

真人平台1.6 ceding: anzhiliangnongduyoudidaogaodeshunxufenbiejiang10μlqianbiaozhunxilierongyehe5μllinsuanerqingan-xiaosuanbarongyetongshizhurushimolu，yuanzihuahouceqixiguangduzhi，yubiaozhunxiliebijiaodingliang。

1.7 jieguojisuan

（ρ-ρ0）×v

真人平台x = ——————————

m×1000

shizhong:

x —yangpinzhongqiandehanliang，mg/100g；

真人平台a —yangpinzhong×××defengmianji；

真人平台ρ —biaozhunrongyezhongqiandezhiliangnongdu，μg/l；

真人平台ρ0 —biaozhunrongyezhong×××××biaozhunpindefengmianji；

m —yangpinzhiliang，g；

v —shiyangxiaohuayededingrongtiji，ml。

1000 -huansuanxishu

2 shendeceding yiju《gb 5009.11》

2.1 yiqi

2.1.1 yuanziyingguangguangpuyi

2.1.2 fenxitianping

真人平台2.1.3 kediaoshidianrelu

2.2 shiji

真人平台2.2.1 qingyanghuana（naoh）

2.2.2 qingyanghuajia（koh）

真人平台2.2.3 pengqinghuajia（kbh4）:fenxichun

真人平台2.2.4 liuniao(ch4n2o2s):fenxichun

2.2.5 yansuan(hcl)

真人平台2.2.6 xiaosuan（hno3）

2.2.7 liusuan（h2so4)

2.2.8 gaolvsuan（hclo4）

2.2.9 xiaosuanmei（[mg(no3)2·6h2o]）: fenxichun

2.2.10 yanghuamei(mgo): fenxichun

2.2.11 kanghuaixuesuan(c6h8o6)

真人平台2.2.12 biaozhunpinlaiyuanchundu: guojiayousejinshujidianzicailiaofenxiceshizhongxin，chundu: 1000 μg/ml。

2.3 seputiaojian

真人平台fugaoya: 260v；shenkongxinyinjidengdianliu: 50ma~80ma: zaiqi: yaqi；zaiqiliusu: 500ml/min；pingbiqiliusu: 800ml/min；celiangfangshi: yingguangqiangdu；dushufangshi: fengmianji。

真人平台2.4 biaozhunpinrongyezhibei:

2.4.1 shenbiaozhunzhongjianye（1.00mg/l）: zhunquexiqushenbiaozhunrongye（1000mg/l）1.00mlyu1000mlrongliangpingzhong，jiaxiaosuanrongye（2+98）zhikedu。

真人平台2.4.2 shenbiaozhunxilierongye: qu25mlrongliangping6zhi，yicizhunquejiarushenbiaozhunzhongjianye（1.00mg/l）0ml、0.10ml、0.25ml、0.50ml、1.50ml、3.00ml（fenbiexiangdangyushennongdu0.0ng/ml、4.0ng/ml、10ng/ml、20ng/ml、60ng/ml、120ng/ml），gejialiusuanrongye（1+9）12.5ml，liuniao+kanghuaixuesuanrongye2ml，bujiashuizhikedu，hunyunhoufangzhi30minhouceding。

真人平台2.5 yangpinrongyezhibei: qugongshipincufenlg ,zhi50mlganguozhong，tongshizuoliangfenshijikongbai。jiaxiaosuan20ml，gaolvsuan4ml，liusuan1.25ml，fangzhiguoye。cirizhiyudianrebanshangjiarexiaojie。jixujiarezhixiaojiewanquan，zaichixuzhengfagaolvsuandebaiyansanjin，liusuandebaiyankaishimaochu。lengquejiashui25ml，zaizhengfazhiliusuanmaobaiyan。lengque，yongshuijiangneirongwuzhuanru25mlrongliangpingzhong，jiaruliuniao+kanghuaixuesuanrongye2ml，bujiashuizhikedu。antongfazuokongbaishiyan。

真人平台2.6ceding: jiangshijikongbai、biaozhunxilierongyeyiciyinruyiqijinxingyuanziyingguangqiangdudeceding。yiyuanziyingguangqiangduweizongzuobiao，shennongduweihengzuobiaohuizhibiaozhunquxian，dedaohuiguifangcheng。xiangtongtiaojianxia，jiangyangpinrongyefenbieyinruyiqijinxingceding。genjuhuiguifangchengjisuanchuyangpinzhongshenyuansudenongdu，jide。

2.7 jieguojisuan

（c-c0）×v×1000

真人平台x = ———————————————

m×1000×1000

shizhong:

真人平台x —yangpinzhongshendehanliang，mg/100g；

c —shiyangbeiceyezhongshendecedingnongdu，ng/ml；

c0 —shiyangkongbaixiaohuayezhongshendecedingnongdu，ng/ml；

v —shiyangxiaohuayezongtiji，ml；

m —yangpinzhiliang，g；

真人平台1000 -huansuanxishu。

真人平台3 gongdeceding yiju《gb 5009.17》

3.1 yiqi

3.1.1 yuanziyingguangguangpuyi

3.1.2 fenxitianping

3.2 shiji

真人平台3.2.1 xiaosuan（hno3）

3.2.2 liusuan（h2so4)

3.2.3 zhonggesuanjia（k2cro7）

3.2.4 biaozhunpinlaiyuanchundu: guojiayousejinshujidianzicailiaofenxiceshizhongxin，chundu: 1000 μg/ml。

3.3 seputiaojian

真人平台guangdianbeizengguanfugaoya: 240v，gongkongxinyinjidengdianliu: 30ma，yuanzihuaqiwendu: 300℃；zaiqiliusu: 500ml/min；pingbiqiliusu: 1000ml/min。

3.4 biaozhunpinrongyezhibei:

3.4.1 gongbiaozhunzhongjianye（10μg/ml）: xiqu1.00mlgongbiaozhunrongye（1.00mg/ml）yu100mlrongliangpingzhong，yongzhonggesuanjiadexiaosuanrongye（0.5g/l）xishizhikedu，hunyun，cirongyedenongduwei10μg/ml，yu4℃bingxiangzhongbiguangbaocun。

3.4.2 gongbiaozhunshiyongye（50ng/ml）: xiqu0.5mldegongbiaozhunzhongjianye（10μg/ml）yu100mlrongliangpingzhong，yongzhonggesuanjiadexiaosuanrongye（0.5g/l）xishizhikedu，hunyun，cirongyedenongduwei50ng/ml，xianyongxianpei

3.4.3 fenbiexiqu50ng/mlgongbiaozhunshiyongye0.00ml、0.20ml、0.50ml、1.00ml、1.50ml、2.00ml、2.50mlyu50mlrongliangpingzhong，yongxiaosuanrongye（1+9）xishizhikedu，yaoyun，gezixiangdangyugongnongduwei0.00ng/ml、0.20ng/ml、0.50ng/ml、1.00ng/ml、1.50ng/ml、2.00ng/ml、2.50ng/ml。

3.5 yangpinrongyezhibei: qugongshipinxifenlg ,zhixiaohuazhuangzhizhuixingpingzhong，jiabolizhushuli，jia45mlxiaosuanhe10mlliusuan，zhuandongzhuixingpingfangzhijubutanhua。zhuangshanglengningguanhou，xiaohuojiare，daikaishifapaotingzhijiare，fapaotingzhihou，jiarehuiliu2xiaoshi。xiaojiedaoyangpinwanquanrongjie，chengwuse，fanglenghouconglengningguanshangduanxiaoxinjia20mlshui，jixujiarehuiliu10fenzhongfangleng，yongshiliangshuichongxilengningguan，chongxiyebingruxiaohuayezhong，jiangxiaohuayejingbolimianguolvyu100mlrongliangpingzhong，yongshaoliangshuixidizhuixingping、lvqi，xidiyebingrurongliangpingnei，jiashuizhikedu，hunyun。tongfazhibeishijikongbairongye。

3.6 ceding: shezhihaoyiqizuijiatiaojian，lianxuyongxiaosuanrongye（1+9）jinyang，daidushuwendinghou，zhuanrubiaozhunxilieceliang，huizhibiaozhunquxian。zhuanrushiyangceliang，xianyongxiaosuanrongye（1+9）jinyang，shidushujibenhuiling，zaifenbiecedingshiyangkongbaiheshiyangxiaohuaye，meicebutongshiyangqiandouyingqingxijinyangqi。shiyangcedingjieguoanshi（1）jisuan。

3.7 jieguojisuan

真人平台（c-c0）×v×1000

真人平台x = ———————————————

m×1000×1000

shizhong:

x—yangpinzhonggongdehanliang，mg/100g；

c —shiyangbeiceyezhonggongdecedingnongdu，ng/ml；

c0 —shiyangkongbaixiaohuayezhonggongdecedingnongdu，ng/ml；

真人平台v --shiyangxiaohuayedingrongzongtiji，ml；

m--yangpinzhiliang，g；

1000--huansuanxishu。

真人平台4 huifendeceding an《gb 5009.04》ceding

4.1 yiqi

4.1.1 mafulu；

真人平台4.1.2 fenxitianping；

真人平台4.1.3 shiyingganguohuociganguo；

4.1.4 ganzaoqi（neiyouganzaoji）；

4.1.5 dianreban

4.2.ganguoyuchuli

qudaxiaoshiyideshiyingganguohuociganguozhigaowenluzhong，zai550℃±25℃xiazhuoshao30min，lengquezhi200℃zuoyou，quchu，fangruganzaoqizhonglengque30min，zhunquechengliang。zhongfuzhuoshaozhiqianhouliangcichengliangxiangchabuchaoguo0.5mgweihengzhong。

4.3 chengyang: zhunquechengquyangpin3g，jingquezhi0.0001g，jiangyangpinjunyunfenbuzaiganguonei，buyaoyajin。

4.4 yangpinchuli: gutishiyangxianzaidianrebanshangxiaohuojiareshishiyangchongfentanhuazhiwuyan，ranhouzhiyugaowenluzhong，zai550℃±25℃xiazhuoshao4h，lengquezhi200℃zuoyou，quchu，fangruganzaoqizhonglengque30min，zhunquechengliang。zhongfuzhuoshaozhiqianhouliangcichengliangxiangchabuchaoguo0.5mgweihengzhong。

真人平台4.5 shiyangzhonghuifendehanliang

m1 - m2

x= —————————— ×100

m3 - m2

shizhong:

真人平台x—yangpinzhonghuifendehanliang，danweiweikemeibaike（g/100g）；

m1—ganguohehuifendezhiliang，danweiweike(g)；

真人平台m2 —ganguodezhiliang，danweiweike(g)；

真人平台m3—ganguoheshiyangdezhiliang，danweiweike(g)；

100--danweihuansuanxishu

【weishengwuzhibiao】yingfuhebiao3deguiding。

biao3 weishengwuzhibiao

xiang  mu	zhi  biao	jiancefangfa
junluozongshu，cfu/g	≤20000	gb 4789.2
dachangjunqun，mpn/g	≤0.92	gb 4789.3 mpn jishufa
meijunhejiaomu，cfu/g	≤50	gb 4789.15
jinhuangseputaoqiujun	≤0/25g	gb 4789.10
shamenshijun	≤0/25g	gb 4789.4

【gongxiaochengfenhuobiaozhixingchengfenzhibiao】yingfuhebiao4deguiding。

biao4 gongxiaochengfenzhibiao

xiang  mu	zhi  biao	jiancefangfa
meipianhan xin（yiznji）	4.5-7.5 mg	gb/t 5009.14
meipianhan yanxianan（yiyanxiananji）	真人平台7.2-16.2 mg	gb/t 5009.89
真人平台meipianhan weishengsuc（yil-kanghuaixuesuanji）	28-63 mg	gb/t 5009.86

真人平台1 xin（zn）hanliangjiance: yiju《gb5009.14》

1.1yuanli: shiyangjingxiaojiechulihou，jinghuoyanyuanzihua，zai213.9nmchucedingxiguangdu。zaiyidingnongdufanweineixindexiguangduzhiyuxinhanliangchengzhengbi，yubiaozhunxiliebijiaodingliang。

1.2shiji

1.2.1 xiaosuan（hno 3）

1.2.2 gaolvsuan（hclo4）

1.2.3biaozhunpinlaiyuanchundu: guojiayousejinshujidianzicailiaoyanjiuzhongxin，chundu: 1000 μg/ml

1.3yiqi

真人平台1.3.1 yuanzixishouguangpuyi: peihuoyanyuanzihuaqi，xinkongxinyinjideng。

1.3.2 fenxitianping: ganliang0.1mghe1mg。

1.3.3 kediaoshidianrelu

1.4 biaozhunquxiandezhibei:

真人平台1.4.1 xinbiaozhunzhongjianye（100mg/l）: zhunquexiquxinbiaozhunrongye（1000mg/l）10mlyu100mlrongliangpingzhong，jiaxiaosuanrongye（5+95）zhikedu，hunyun。

真人平台1.4.2 xinbiaozhunxilierongye: fenbiexiquxinbiaozhunzhongjianye（100μg/ml）0ml，1.00ml，2.00ml，4.00ml，8.00ml，10mlyu100mlrongliangpingzhong，jiaxiaosuanrongye（5+95）dingrongzhikedu，hunyun。zhichengxinzhiliangnongduwei0μg/ml、1.00μg/ml、2.00μg/ml、4.00μg/ml、8.00μg/ml、10.00μg/mldebiaozhunxilierongye。

1.5 yangpinchuli

qubenpinxifen0.5g，zhi150mlzhuixingpingzhong，jia10mlxiaosuan、0.5mlgaolvsuan，zaikediaoshidianrelushangxiaojie。ruoxiaohuayechengzonghese，zaijiaxiaosuan，xiaojiezhimaobaiyan，xiaohuayechenghuangsetouming。quchuzhuixingping，lengquehouyongshuizhuanyizhi1000mlrongliangpingzhong，yongshaoliangshuixidi2~3ci，hebingxidiyeyurongliangpingzhongbingyongshuidingrongzhikedu，hunyunbeiyong。tongshizuoshijikongbaishiyan。

真人平台1.6 yangpinceding: jiangxinbiaozhunxilierongyeannongduyoudidaogaodeshunxudaoruhuoyanyuanzihuaqi，zai213.9nmdebozhangchucedingxiguangdu，yixindezhiliangnongduweihengzuobiao，xiangyingdexiguangduzhiweizongzuobiao，zhizuobiaozhunquxian。tongfacedingkongbairongyeheshiyangdaiceyedexiguangduzhi，yubiaozhunxiliebijiaodingliang。

1.7 jieguojisuan

真人平台(ρ-ρ 0)×v×s×1000

x = ——————————

m×1000×1000

shizhong:

x —yangpinzhongxindehanliang，mg/pian；

ρ—yangpincedingyezhongxindezhiliangnongdu,μg/ml；

ρ0 —yangpinkongbaiyezhongxindezhiliangnongdu，μg/ml；

真人平台m —yangpinzhiliang，danweiweig；

真人平台v —shiyangxiaohuayedingrongtiji，ml；

s —pingjunpianzhong，danweiweig；

真人平台1000 —danweihuansuanxishu。

真人平台2 yanxiananhanliangjiance: yiju《gb5009.89》

2.1 yuanli: gaodanbaiyangpinjingchendiandanbaizhi，gaodianfenyangpinjingdianfenmeimeijie，zairuosuanhuanjingxiachaoshengbozhendangtiqu，yic 18 sepuzhufenli，zaiziwaijianceqijiance261nmbozhangchujiance，genjusepuzhudebaoliushijiandingxing，waibiaofadingliang，jisuanshiyangzhongyansuanheyanxianandehanliang。

2.2 shiji

2.2.1 yansuan（hcl）: youjichun。

2.2.2qingyanghuana（naoh）: youjichun。

真人平台2.2.3gaolvsuan（hclo 4）: youjichun。

真人平台2.2.4jiachun（ch 3oh）: sepuchun。

真人平台2.2.5yibingchun（c 3h 8o）: sepuchun。

2.2.6gengwanhuangsuanna（c 7h 15nao 3s）: sepuchun。

真人平台2.2.7 biaozhunpinlaiyuanchundu: zhongjianyuan，chundu99.9%

2.3 yiqi

2.3.1gaoxiaoyexiangsepuyi: daiziwaijianceqi，。

2.3.2fenxitianping: ganliang0.1mg。

2.3.3 chaoshengbozhendangqi。

真人平台2.3.4 phji: jingdu±0.01。

2.4 seputiaojian

a)sepuzhu: c18(zhuzhang250mm，neijing4.6mm，lijing5 μm)

b)zhuwen: 25℃±0.5℃。

c)liudongxiang: jiachun70ml、yibingchun20ml、gengwanhuangsuanna1g，yong910mlshuirongjiebinghunyunhou，yonggaolvsuandiaophzhi2.1±0.1，jing0.45μmmoguolv。

真人平台d)liusu: 1.0 ml/min

e)ziwaijiancebozhang: 261m

f)jinyangliang: 10μl

2.5 biaozhunquxiandezhibei:

2.5.1yanxiananbiaozhunchubeiye（1.000mg/ml）: zhunquechengquyanxiananbiaozhunpin0.05g（jingquedao0.1mg）yu100mlrongliangpingzhong，yong0.1mol/l)yansuanrongjie，dingrongzhikedu，hunyun。

2.5.2yanxiananbiaozhunzhongjianrongye（100μg/ml）: zhunquexiquyanxiananbiaozhunchubeiye10.0mlyu100mlrongliangpingzhong，jiashuidingrongzhikedu，hunyun，linyongqianpeizhi。

2.5.3yanxiananbiaozhungongzuoye: zhunquexiqubiaozhunzhongjianye: 1.0ml、2.0ml、5.0ml、10.0ml、20.0mlyu100mlrongliangpingzhong，jiashuidingrongzhikedu，hunyun，dedaonongdufenbiewei1.0μg/ml、2.0μg/ml、5.0μg/ml、10.0μg/ml、20.0μg/mldebiaozhungongzuoye。linyongqianpeizhi。

2.6yangpinchuli

qubenpinxifen4g（jingquedao0.01g），jiaruyue25ml45℃~50℃deshui，zhiyuchaoshengbozhendangqizhongzhendangyue10minyishangchongfenrongjie，jingzhi5min~10min，binglengquezhishiwen。yong5.0mol/lyansuanrongyehe0.1mol/lyansuanrongyediaojieshiyangrongyedephzhi1.7±0.1，fangzhiyue2minhou，zaiyong5.0mol/lqingyanghuanarongyehe0.1mol/lqingyanghuanarongyediaojieshiyangrongyedephzhi4.5±0.1，zhiyu50℃shuiyuchaoshengbozhendang10minyishangchongfentiqu，lengquezhishiwenhouzhuanzhi100mlrongliangpingzhong，yongshuifanfuchongxizhuixingping，xiyehebingyu100mlrongliangpingzhong，yongshuidingrongzhikeduhouhunyun，zaixiqu1mlzhi100mlrongliangpingzhong，yongshuixishizhikedu，jinglvzhiguolv，lvyezaijing0.45μmweikonglvmojiayaguolv，jiweishiyangcedingye。

2.7 yangpinceding: jiangyanxiananbiaozhunxiliecedingyeyicianzhaoshangshuseputiaojianjinxingceding，jilusepufengmianji，yifengmianjiweizongzuobiao，yibiaozhuncedingyedenongduweihengzuobiao，huizhibiaozhunquxian。zaijiangshiyangcedingyeanzhaoshangshuseputiaojianjinxingceding，jilusepufengmianji，genjubiaozhunquxianjisuanchushiyangcedingyezhongyanxianandenongdu。

2.8 jieguojisuan

ρ×v×s×1000

x = ——————————

真人平台m×1000×1000

shizhong:

x —yangpinzhongyanxianandehanliang，danweiweihaokemeipian（mg/pian）；

真人平台ρ—congbiaozhunquxianshangchadedeyanxianandenongdu，danweiweiweikemeihaosheng（μg/ml）；

真人平台v—dingrongtiji，danweiweihaosheng（ml）；

真人平台s—pingjunpianzhong，danweiweike（g）；

m—shiyangdechengyangliang，danweiweike（g）；

1000—danweihuansuanxishu。

3 weishengsuchanliangjiance yiju《gb 5009.86》

3.1 yuanli: shiyangzhongdekanghuaixuesuanyongpianlinsuanrongjiechaoshengtiquhou，yiliziduishijiweiliudongxiang，jingfanxiangsepuzhufenli，yongpeiyouziwaijianceqideyexiangsepuyijiance。yisepufengbaoliushijiandingxing，waibiaofadingliang。

3.2 shiji

3.2.1pianlinsuan（hpo 3）n: hanliang（yihpo 3ji）≥38%。

3.2.2 linsuanerqingjia（kh 2po 4）

3.2.3shiliuwanjisanjiajixiuhuaan（c 19h 42brn）: sepuchun

真人平台3.2.4jiachun（ch 3oh）: sepuchun

3.2.5 biaozhunpinlaiyuanchundu: zhongjianyuan，chundu100%。

3.3yiqi

真人平台3.3.1gaoxiaoyexiangsepuyi: peiyouziwaijianceqi。

真人平台3.3.2 phji: jingdu±0.01。

真人平台3.3.3fenxitianping: ganliangwei0.1g、1mg、0.01mg。

3.3.4chaoshengboqingxiqi

真人平台3.3.5lixinji: zhuansu≥4000 r/min。

3.4 seputiaojian

a)sepuzhu: c18(zhuzhang250mm，neijing4.6mm，lijing5 μm)

b)zhuwen: 25℃

c)liudongxiang: a: 6.8glinsuanerqingjiahe0.91gshiliuwanjisanjiajixiuhuaan，yongshuirongjiebingdingrongzhi1l（yonglinsuandiaophzhi2.5~2.8）；b；100%jiachun。ana: b=98: 2hunhe，guo0.45μmlvmo，chaoshengtuoqi。

真人平台d)liusu: 0.7ml/min

e)ziwaijiancebozhang: 245nm

f)jinyangliang: 20μl

3.5 biaozhunquxiandezhibei:

真人平台3.5.1 l（+）kanghuaixuesuanbiaozhunchubeirongye（1.000mg/ml）: zhunquechengqubiaozhunpinl（+）kanghuaixuesuan0.01g（jingquezhi0.01mg），yong20g/ldepianlinsuanrongyedingrongzhi10ml。

1.5.2 l（+）kanghuaixuesuanbiaozhunxiliegongzuorongye: fenbiezhunquexiqul（+）kanghuaixuesuanbiaozhunrongyezhongjianye0.ml，0.05ml，0.50ml，1.0ml，2.5ml，5.0ml，yong20g/ldepianlinsuanrongyedingrongzhi100ml。biaozhunxiliegongzuorongyedefenbienongduwei0μg/ml、0.5μg/ml、5.0μg/ml、10.0μg/ml、25.00μg/ml、50.0μg/ml。

3.6 yangpinchuli

qubenpinshiliang，yanxi，jingmichengding0.5g（jingquezhi0.001g），yong20g/ldepianlinsuanrongyejiangshiyangzhuanyizhi50mlrongliangpingzhong。zhenyaorongjiebingdingrong。yaoyun，quanbuzhuanyizhi50mllixinguanzhong，chaoshengtiqu5fenzhonghou，yu4000r/minlixin5min，qushangqingyeguo0.45μmshuixianglvmo，zuoweigongshipinrongye。

真人平台3.7 yangpinceding: fenbiexiqul（+）kanghuaixuesuanbiaozhunxiliegongzuorongye10μlzhurugaoxiaoyexiangsepuyizhong，cedingxiangyingdefengmianji，yifengmianjiweizongzuobiao，yibiaozhuncedingyenongduweihengzuobiaohuizhibiaozhunquxian，jisuanhuiguifangcheng。gongshipinjinggaoxiaoyexiangsepuyifenxi，cedefengmianji，caiyongwaibiaofatongguoshangshubiaozhunquxianjisuanqinongdu。

3.8 jieguojisuan

ρ×v×s×1000

x = ——————————

真人平台m×1000×1000

shizhong:

真人平台x—yangpinzhongkanghuaixuesuandehanliang，danweiweihaokemeipian（mg/pian）；

ρ —congbiaozhunquxianshangchadedekanghuaixuesuandenongdu，danweiweiweikemeihaosheng（μg/ml）；

v—dingrongtiji，danweiweihaosheng（ml）；

真人平台s—pingjunpianzhong，danweiweike（g）；

真人平台m—shiyangdechengyangliang，danweiweike（g）；

1000—danweihuansuanxishu。

【zhongliangchayizhibiao】

yingfuhe《zhonghuarenmingongheguoyaodian》zhong“zhijitongze”xiangxiapianjideguiding。

【yuanfuliaozhiliangyaoqiu】

1、rusuanxin: yingfuhegb 1903.11 《shipinanquanguojiabiaozhun shipinyingyangqianghuaji rusuanxin》deguiding

2、yanxianan: yingfuhezhongguoyaodian《yanxianan》deguiding

3、l-kanghuaixuesuan: yingfuhegb 14754 《shipinanquanguojiabiaozhun shipintianjiaji weishengsuc（kanghuaixuesuan）》deguiding

4、zhetang: yingfuhexianxing《zhonghuarenmingongheguoyaodian》deguiding

真人平台5、d-ganlutangchun: yingfuhegb 1886.177 《shipinanquanguojiabiaozhun shipintianjiaji d-ganlutangchun》deguiding

真人平台6、maiyahujing: yingfuhegb/t 20884 《maiyahujing》deguiding

7、rutang: yingfuhegb25595 《shipinanquanguojiabiaozhun rutang 》deguiding