真人平台

国产保健食品备案凭证(千雌愫牌锌烟酸维生素C咀嚼片)

真人平台  fabushijian: 2019-11-25 09:55:06  

chanpinmingcheng

真人平台qiancisupaixinyansuanweishengsucjujiaopian

beianren

shanxidetongbaoyiyaokejiyouxiangongsi

beianrendizhi

真人平台shanxishengxianshigaoxinquxinxinggongyeyuanchuangyedadao22haobangonglou3lou301shi

beianjielun

anzhao《zhonghuarenmingongheguoshipinanquanfa》《baojianshipinzhuceyubeianguanlibanfa》dengfalv、guizhangdeguiding,yuyibeian。

beianhao

shijianbeig202061001898

fujian

1 chanpinshuomingshu;2 chanpinjishuyaoqiu

beizhu

真人平台2020nian11yue03ri

fujian1

baojianshipinchanpinshuomingshu

shijianbeig202061001898

───────────────────────────────────────────

真人平台qiancisupaixinyansuanweishengsucjujiaopian

真人平台【yuanliao】rusuanxin,yanxianan,l-kanghuaixuesuan

【fuliao】zhetang,d-ganlutangchun,maiyahujing,rutang

【gongxiaochengfenjihanliang】meipianhan: xin 6mg yanxianan 9mg weishengsuc 35mg

【shiyirenqun】xuyaobuchongxin、yanxianan、weishengsucde chengren

真人平台【bushiyirenqun】17suiyixiarenqunjiyunfu、rumu

真人平台【baojiangongneng】buchongxin、yansuan、weishengsuc

真人平台【shiyongliangjishiyongfangfa】meiri 1 ci, meici 2 pian,shiyongfangfa: jujiaoshiyong

【guige】1.0 g/pian

真人平台【zhuzangfangfa】mifeng,yinliangganzaochubaocun

【baozhiqi】24geyue

【zhuyishixiang】benpinbunengdaitiyaowu。shiyirenqunwaiderenqunbutuijianshiyongbenchanpin。buyichaoguotuijianlianghuoyutongleiyingyangsutongshishiyong

fujian2

baojianshipinchanpinjishuyaoqiu

shijianbeig202061001898

真人平台───────────────────────────────────────────

真人平台qiancisupaixinyansuanweishengsucjujiaopian

真人平台【yuanliao】rusuanxin,yanxianan,l-kanghuaixuesuan

【fuliao】zhetang,d-ganlutangchun,maiyahujing,rutang

真人平台【shengchangongyi】benpinjingganzao(50℃)dengzhuyaogongyijiagongzhicheng。

真人平台【zhijiejiechuchanpinbaozhuangcailiaodezhonglei、mingchengjibiaozhun】

真人平台gutiyaoyonggaomidujuyixipingyingfuhe《koufugutiyaoyonggaomidujuyixiping》(ybb 00122002);suliaofangdaopinggaiyingfuhe《baozhuangrongqi suliaofangdaopinggai》(gb/t 17876)。

真人平台【ganguanyaoqiu】yingfuhebiao1deguiding。

biao 1 ganguanyaoqiu

xiang  mu

zhi  biao

se ze

rubaisezhibaise

ziwei、qiwei

weisuanweitian、wuyiwei

zhuang tai

wuzhengchangshilikejianwailaizazhi

【jianbie】

wu

【lihuazhibiao】yingfuhebiao2deguiding。

biao2 lihuazhibiao

xiang  mu

zhi  biao

jiancefangfa

qian(yi pbji),mg/kg

≤2.0

gb 5009.12

zongshen(yi asji),mg/kg

≤1.0

gb 5009.11

zonggong(yi hgji),mg/kg

≤0.3

gb 5009.17

huifen,%

≤9

gb 5009.4

1 qiandeceding yiju《gb 5009.12》

1.1 yiqi

真人平台1.1.1 yuanzixishouguangpuyi: peishimoluyuanzihuaqi,fuqiankongxinyinjideng

1.1.2 fenxitianping

1.1.3 kediaoshidianrelu

1.2 shiji

真人平台1.2.1 xiaosuan(hno3)。

1.2.2 gaolvsuan(hclo4)

真人平台1.2.3 linsuanerqingan(nh4h2po4)

1.2.4 xiaosuanba(pd(no3)2)

真人平台1.2.5 biaozhunpinlaiyuanchundu: guojiayousejinshujidianzicailiaofenxiceshizhongxin,chundu: 1000 μg/ml。

1.3 yiqitiaojian;

真人平台bozhang283.3nm;xiafeng0.5nm;dengdianliu8~12mv;

ganzao: 85℃~120℃/40s~50s;huihua: 750℃/20s~30s;yuanzihua: 2300℃/4s~5s。

真人平台1.4 biaozhunpinrongyezhibei:

真人平台1.4.1 qianbiaozhunzhongjianye(1.00mg/l): zhunquexiquqianbiaozhunrongye(1000mg/l)1.00mlyu1000mlrongliangpingzhong,jiaxiaosuanrongye(5+95)zhikedu。

1.4.2 qianbiaozhunxilierongye: fenbiexiquqianbiaozhunzhongjianye(1.00mg/l)0ml、0.500ml、1.00ml、2.00ml、3.00ml、4.00mlyu100mlrongliangpingzhong,jiaxiaosuanrongye(5+95)zhikedu,hunyun。ciqianbiaozhunxilierongyedenongdufenbieweiqian0µg/l、5µg/l、10µg/l、20µg/l、30µg/l、40µg/l。

1.5 yangpinrongyezhibei: chengqugutishiyang1gyuzhuixingpingzhong,jia10mlxiaosuan、0.5mlgaolvsuan,zaikediaoshidianrelushangxiaojie。ruoxiaohuayechengzonghese,zaijiaxiaosuan,xiaojiezhimaobaiyan,xiaohuayechengwusetouminghuolvedaihuangse。quchuzhuixingping,lengquehouyongshuizhuanyizhi10mlrongliangpingzhong,hunyunbeiyong。tongshizuoshijikongbaishiyan

真人平台1.6 ceding: anzhiliangnongduyoudidaogaodeshunxufenbiejiang10μlqianbiaozhunxilierongyehe5μllinsuanerqingan-xiaosuanbarongyetongshizhurushimolu,yuanzihuahouceqixiguangduzhi,yubiaozhunxiliebijiaodingliang。

1.7 jieguojisuan

(ρ-ρ0)×v

真人平台x = ——————————

m×1000

shizhong:

x —yangpinzhongqiandehanliang,mg/100g;

真人平台a —yangpinzhong×××defengmianji;

真人平台ρ —biaozhunrongyezhongqiandezhiliangnongdu,μg/l;

真人平台ρ0 —biaozhunrongyezhong×××××biaozhunpindefengmianji;

m —yangpinzhiliang,g;

v —shiyangxiaohuayededingrongtiji,ml。

1000 -huansuanxishu

2 shendeceding yiju《gb 5009.11》

2.1 yiqi

2.1.1 yuanziyingguangguangpuyi

2.1.2 fenxitianping

真人平台2.1.3 kediaoshidianrelu

2.2 shiji

真人平台2.2.1 qingyanghuana(naoh)

2.2.2 qingyanghuajia(koh)

真人平台2.2.3 pengqinghuajia(kbh4):fenxichun

真人平台2.2.4 liuniao(ch4n2o2s):fenxichun

2.2.5 yansuan(hcl)

真人平台2.2.6 xiaosuan(hno3)

2.2.7 liusuan(h2so4)

2.2.8 gaolvsuan(hclo4)

2.2.9 xiaosuanmei([mg(no3)2·6h2o]): fenxichun

2.2.10 yanghuamei(mgo): fenxichun

2.2.11 kanghuaixuesuan(c6h8o6)

真人平台2.2.12 biaozhunpinlaiyuanchundu: guojiayousejinshujidianzicailiaofenxiceshizhongxin,chundu: 1000 μg/ml。

2.3 seputiaojian

真人平台fugaoya: 260v;shenkongxinyinjidengdianliu: 50ma~80ma: zaiqi: yaqi;zaiqiliusu: 500ml/min;pingbiqiliusu: 800ml/min;celiangfangshi: yingguangqiangdu;dushufangshi: fengmianji。

真人平台2.4 biaozhunpinrongyezhibei:

2.4.1 shenbiaozhunzhongjianye(1.00mg/l): zhunquexiqushenbiaozhunrongye(1000mg/l)1.00mlyu1000mlrongliangpingzhong,jiaxiaosuanrongye(2+98)zhikedu。

真人平台2.4.2 shenbiaozhunxilierongye: qu25mlrongliangping6zhi,yicizhunquejiarushenbiaozhunzhongjianye(1.00mg/l)0ml、0.10ml、0.25ml、0.50ml、1.50ml、3.00ml(fenbiexiangdangyushennongdu0.0ng/ml、4.0ng/ml、10ng/ml、20ng/ml、60ng/ml、120ng/ml),gejialiusuanrongye(1+9)12.5ml,liuniao+kanghuaixuesuanrongye2ml,bujiashuizhikedu,hunyunhoufangzhi30minhouceding。

真人平台2.5 yangpinrongyezhibei: qugongshipincufenlg ,zhi50mlganguozhong,tongshizuoliangfenshijikongbai。jiaxiaosuan20ml,gaolvsuan4ml,liusuan1.25ml,fangzhiguoye。cirizhiyudianrebanshangjiarexiaojie。jixujiarezhixiaojiewanquan,zaichixuzhengfagaolvsuandebaiyansanjin,liusuandebaiyankaishimaochu。lengquejiashui25ml,zaizhengfazhiliusuanmaobaiyan。lengque,yongshuijiangneirongwuzhuanru25mlrongliangpingzhong,jiaruliuniao+kanghuaixuesuanrongye2ml,bujiashuizhikedu。antongfazuokongbaishiyan。

真人平台2.6ceding: jiangshijikongbai、biaozhunxilierongyeyiciyinruyiqijinxingyuanziyingguangqiangdudeceding。yiyuanziyingguangqiangduweizongzuobiao,shennongduweihengzuobiaohuizhibiaozhunquxian,dedaohuiguifangcheng。xiangtongtiaojianxia,jiangyangpinrongyefenbieyinruyiqijinxingceding。genjuhuiguifangchengjisuanchuyangpinzhongshenyuansudenongdu,jide。

2.7 jieguojisuan

(c-c0)×v×1000

真人平台x = ———————————————

m×1000×1000

shizhong:

真人平台x —yangpinzhongshendehanliang,mg/100g;

c —shiyangbeiceyezhongshendecedingnongdu,ng/ml;

c0 —shiyangkongbaixiaohuayezhongshendecedingnongdu,ng/ml;

v —shiyangxiaohuayezongtiji,ml;

m —yangpinzhiliang,g;

真人平台1000 -huansuanxishu。

真人平台3 gongdeceding yiju《gb 5009.17》

3.1 yiqi

3.1.1 yuanziyingguangguangpuyi

3.1.2 fenxitianping

3.2 shiji

真人平台3.2.1 xiaosuan(hno3)

3.2.2 liusuan(h2so4)

3.2.3 zhonggesuanjia(k2cro7)

3.2.4 biaozhunpinlaiyuanchundu: guojiayousejinshujidianzicailiaofenxiceshizhongxin,chundu: 1000 μg/ml。

3.3 seputiaojian

真人平台guangdianbeizengguanfugaoya: 240v,gongkongxinyinjidengdianliu: 30ma,yuanzihuaqiwendu: 300℃;zaiqiliusu: 500ml/min;pingbiqiliusu: 1000ml/min。

3.4 biaozhunpinrongyezhibei:

3.4.1 gongbiaozhunzhongjianye(10μg/ml): xiqu1.00mlgongbiaozhunrongye(1.00mg/ml)yu100mlrongliangpingzhong,yongzhonggesuanjiadexiaosuanrongye(0.5g/l)xishizhikedu,hunyun,cirongyedenongduwei10μg/ml,yu4℃bingxiangzhongbiguangbaocun。

3.4.2 gongbiaozhunshiyongye(50ng/ml): xiqu0.5mldegongbiaozhunzhongjianye(10μg/ml)yu100mlrongliangpingzhong,yongzhonggesuanjiadexiaosuanrongye(0.5g/l)xishizhikedu,hunyun,cirongyedenongduwei50ng/ml,xianyongxianpei

3.4.3 fenbiexiqu50ng/mlgongbiaozhunshiyongye0.00ml、0.20ml、0.50ml、1.00ml、1.50ml、2.00ml、2.50mlyu50mlrongliangpingzhong,yongxiaosuanrongye(1+9)xishizhikedu,yaoyun,gezixiangdangyugongnongduwei0.00ng/ml、0.20ng/ml、0.50ng/ml、1.00ng/ml、1.50ng/ml、2.00ng/ml、2.50ng/ml。

3.5 yangpinrongyezhibei: qugongshipinxifenlg ,zhixiaohuazhuangzhizhuixingpingzhong,jiabolizhushuli,jia45mlxiaosuanhe10mlliusuan,zhuandongzhuixingpingfangzhijubutanhua。zhuangshanglengningguanhou,xiaohuojiare,daikaishifapaotingzhijiare,fapaotingzhihou,jiarehuiliu2xiaoshi。xiaojiedaoyangpinwanquanrongjie,chengwuse,fanglenghouconglengningguanshangduanxiaoxinjia20mlshui,jixujiarehuiliu10fenzhongfangleng,yongshiliangshuichongxilengningguan,chongxiyebingruxiaohuayezhong,jiangxiaohuayejingbolimianguolvyu100mlrongliangpingzhong,yongshaoliangshuixidizhuixingping、lvqi,xidiyebingrurongliangpingnei,jiashuizhikedu,hunyun。tongfazhibeishijikongbairongye。

3.6 ceding: shezhihaoyiqizuijiatiaojian,lianxuyongxiaosuanrongye(1+9)jinyang,daidushuwendinghou,zhuanrubiaozhunxilieceliang,huizhibiaozhunquxian。zhuanrushiyangceliang,xianyongxiaosuanrongye(1+9)jinyang,shidushujibenhuiling,zaifenbiecedingshiyangkongbaiheshiyangxiaohuaye,meicebutongshiyangqiandouyingqingxijinyangqi。shiyangcedingjieguoanshi(1)jisuan。

3.7 jieguojisuan

真人平台(c-c0)×v×1000

真人平台x = ———————————————

m×1000×1000

shizhong:

x—yangpinzhonggongdehanliang,mg/100g;

c —shiyangbeiceyezhonggongdecedingnongdu,ng/ml;

c0 —shiyangkongbaixiaohuayezhonggongdecedingnongdu,ng/ml;

真人平台v --shiyangxiaohuayedingrongzongtiji,ml;

m--yangpinzhiliang,g;

1000--huansuanxishu。

真人平台4 huifendeceding an《gb 5009.04》ceding

4.1 yiqi

4.1.1 mafulu;

真人平台4.1.2 fenxitianping;

真人平台4.1.3 shiyingganguohuociganguo;

4.1.4 ganzaoqi(neiyouganzaoji);

4.1.5 dianreban

4.2.ganguoyuchuli

qudaxiaoshiyideshiyingganguohuociganguozhigaowenluzhong,zai550℃±25℃xiazhuoshao30min,lengquezhi200℃zuoyou,quchu,fangruganzaoqizhonglengque30min,zhunquechengliang。zhongfuzhuoshaozhiqianhouliangcichengliangxiangchabuchaoguo0.5mgweihengzhong。

4.3 chengyang: zhunquechengquyangpin3g,jingquezhi0.0001g,jiangyangpinjunyunfenbuzaiganguonei,buyaoyajin。

4.4 yangpinchuli: gutishiyangxianzaidianrebanshangxiaohuojiareshishiyangchongfentanhuazhiwuyan,ranhouzhiyugaowenluzhong,zai550℃±25℃xiazhuoshao4h,lengquezhi200℃zuoyou,quchu,fangruganzaoqizhonglengque30min,zhunquechengliang。zhongfuzhuoshaozhiqianhouliangcichengliangxiangchabuchaoguo0.5mgweihengzhong。

真人平台4.5 shiyangzhonghuifendehanliang

m1 - m2

x= —————————— ×100

m3 - m2

shizhong:

真人平台x—yangpinzhonghuifendehanliang,danweiweikemeibaike(g/100g);

m1—ganguohehuifendezhiliang,danweiweike(g);

真人平台m2 —ganguodezhiliang,danweiweike(g);

真人平台m3—ganguoheshiyangdezhiliang,danweiweike(g);

100--danweihuansuanxishu

【weishengwuzhibiao】yingfuhebiao3deguiding。

biao3 weishengwuzhibiao

xiang  mu

zhi  biao

jiancefangfa

junluozongshu,cfu/g

≤20000

gb 4789.2

dachangjunqun,mpn/g

≤0.92

gb 4789.3 mpn jishufa

meijunhejiaomu,cfu/g

≤50

gb 4789.15

jinhuangseputaoqiujun

≤0/25g

gb 4789.10

shamenshijun

≤0/25g

gb 4789.4

【gongxiaochengfenhuobiaozhixingchengfenzhibiao】yingfuhebiao4deguiding。

biao4 gongxiaochengfenzhibiao

xiang  mu

zhi  biao

jiancefangfa

meipianhan xin(yiznji)

4.5-7.5 mg

gb/t 5009.14

meipianhan yanxianan(yiyanxiananji)

真人平台7.2-16.2 mg

gb/t 5009.89

真人平台meipianhan weishengsuc(yil-kanghuaixuesuanji)

28-63 mg

gb/t 5009.86

真人平台1 xin(zn)hanliangjiance: yiju《gb5009.14》

1.1yuanli: shiyangjingxiaojiechulihou,jinghuoyanyuanzihua,zai213.9nmchucedingxiguangdu。zaiyidingnongdufanweineixindexiguangduzhiyuxinhanliangchengzhengbi,yubiaozhunxiliebijiaodingliang。

1.2shiji

1.2.1 xiaosuan(hno 3)

1.2.2 gaolvsuan(hclo4)

1.2.3biaozhunpinlaiyuanchundu: guojiayousejinshujidianzicailiaoyanjiuzhongxin,chundu: 1000 μg/ml

1.3yiqi

真人平台1.3.1 yuanzixishouguangpuyi: peihuoyanyuanzihuaqi,xinkongxinyinjideng。

1.3.2 fenxitianping: ganliang0.1mghe1mg。

1.3.3 kediaoshidianrelu

1.4 biaozhunquxiandezhibei:

真人平台1.4.1 xinbiaozhunzhongjianye(100mg/l): zhunquexiquxinbiaozhunrongye(1000mg/l)10mlyu100mlrongliangpingzhong,jiaxiaosuanrongye(5+95)zhikedu,hunyun。

真人平台1.4.2 xinbiaozhunxilierongye: fenbiexiquxinbiaozhunzhongjianye(100μg/ml)0ml,1.00ml,2.00ml,4.00ml,8.00ml,10mlyu100mlrongliangpingzhong,jiaxiaosuanrongye(5+95)dingrongzhikedu,hunyun。zhichengxinzhiliangnongduwei0μg/ml、1.00μg/ml、2.00μg/ml、4.00μg/ml、8.00μg/ml、10.00μg/mldebiaozhunxilierongye。

1.5 yangpinchuli

qubenpinxifen0.5g,zhi150mlzhuixingpingzhong,jia10mlxiaosuan、0.5mlgaolvsuan,zaikediaoshidianrelushangxiaojie。ruoxiaohuayechengzonghese,zaijiaxiaosuan,xiaojiezhimaobaiyan,xiaohuayechenghuangsetouming。quchuzhuixingping,lengquehouyongshuizhuanyizhi1000mlrongliangpingzhong,yongshaoliangshuixidi2~3ci,hebingxidiyeyurongliangpingzhongbingyongshuidingrongzhikedu,hunyunbeiyong。tongshizuoshijikongbaishiyan。

真人平台1.6 yangpinceding: jiangxinbiaozhunxilierongyeannongduyoudidaogaodeshunxudaoruhuoyanyuanzihuaqi,zai213.9nmdebozhangchucedingxiguangdu,yixindezhiliangnongduweihengzuobiao,xiangyingdexiguangduzhiweizongzuobiao,zhizuobiaozhunquxian。tongfacedingkongbairongyeheshiyangdaiceyedexiguangduzhi,yubiaozhunxiliebijiaodingliang。

1.7 jieguojisuan

真人平台(ρ-ρ 0)×v×s×1000

x = ——————————

m×1000×1000

shizhong:

x —yangpinzhongxindehanliang,mg/pian;

ρ—yangpincedingyezhongxindezhiliangnongdu,μg/ml;

ρ0 —yangpinkongbaiyezhongxindezhiliangnongdu,μg/ml;

真人平台m —yangpinzhiliang,danweiweig;

真人平台v —shiyangxiaohuayedingrongtiji,ml;

s —pingjunpianzhong,danweiweig;

真人平台1000 —danweihuansuanxishu。

真人平台2 yanxiananhanliangjiance: yiju《gb5009.89》

2.1 yuanli: gaodanbaiyangpinjingchendiandanbaizhi,gaodianfenyangpinjingdianfenmeimeijie,zairuosuanhuanjingxiachaoshengbozhendangtiqu,yic 18 sepuzhufenli,zaiziwaijianceqijiance261nmbozhangchujiance,genjusepuzhudebaoliushijiandingxing,waibiaofadingliang,jisuanshiyangzhongyansuanheyanxianandehanliang。

2.2 shiji

2.2.1 yansuan(hcl): youjichun。

2.2.2qingyanghuana(naoh): youjichun。

真人平台2.2.3gaolvsuan(hclo 4): youjichun。

真人平台2.2.4jiachun(ch 3oh): sepuchun。

真人平台2.2.5yibingchun(c 3h 8o): sepuchun。

2.2.6gengwanhuangsuanna(c 7h 15nao 3s): sepuchun。

真人平台2.2.7 biaozhunpinlaiyuanchundu: zhongjianyuan,chundu99.9%

2.3 yiqi

2.3.1gaoxiaoyexiangsepuyi: daiziwaijianceqi,。

2.3.2fenxitianping: ganliang0.1mg。

2.3.3 chaoshengbozhendangqi。

真人平台2.3.4 phji: jingdu±0.01。

2.4 seputiaojian

a)sepuzhu: c18(zhuzhang250mm,neijing4.6mm,lijing5 μm)

b)zhuwen: 25℃±0.5℃。

c)liudongxiang: jiachun70ml、yibingchun20ml、gengwanhuangsuanna1g,yong910mlshuirongjiebinghunyunhou,yonggaolvsuandiaophzhi2.1±0.1,jing0.45μmmoguolv。

真人平台d)liusu: 1.0 ml/min

e)ziwaijiancebozhang: 261m

f)jinyangliang: 10μl

2.5 biaozhunquxiandezhibei:

2.5.1yanxiananbiaozhunchubeiye(1.000mg/ml): zhunquechengquyanxiananbiaozhunpin0.05g(jingquedao0.1mg)yu100mlrongliangpingzhong,yong0.1mol/l)yansuanrongjie,dingrongzhikedu,hunyun。

2.5.2yanxiananbiaozhunzhongjianrongye(100μg/ml): zhunquexiquyanxiananbiaozhunchubeiye10.0mlyu100mlrongliangpingzhong,jiashuidingrongzhikedu,hunyun,linyongqianpeizhi。

2.5.3yanxiananbiaozhungongzuoye: zhunquexiqubiaozhunzhongjianye: 1.0ml、2.0ml、5.0ml、10.0ml、20.0mlyu100mlrongliangpingzhong,jiashuidingrongzhikedu,hunyun,dedaonongdufenbiewei1.0μg/ml、2.0μg/ml、5.0μg/ml、10.0μg/ml、20.0μg/mldebiaozhungongzuoye。linyongqianpeizhi。

2.6yangpinchuli

qubenpinxifen4g(jingquedao0.01g),jiaruyue25ml45℃~50℃deshui,zhiyuchaoshengbozhendangqizhongzhendangyue10minyishangchongfenrongjie,jingzhi5min~10min,binglengquezhishiwen。yong5.0mol/lyansuanrongyehe0.1mol/lyansuanrongyediaojieshiyangrongyedephzhi1.7±0.1,fangzhiyue2minhou,zaiyong5.0mol/lqingyanghuanarongyehe0.1mol/lqingyanghuanarongyediaojieshiyangrongyedephzhi4.5±0.1,zhiyu50℃shuiyuchaoshengbozhendang10minyishangchongfentiqu,lengquezhishiwenhouzhuanzhi100mlrongliangpingzhong,yongshuifanfuchongxizhuixingping,xiyehebingyu100mlrongliangpingzhong,yongshuidingrongzhikeduhouhunyun,zaixiqu1mlzhi100mlrongliangpingzhong,yongshuixishizhikedu,jinglvzhiguolv,lvyezaijing0.45μmweikonglvmojiayaguolv,jiweishiyangcedingye。

2.7 yangpinceding: jiangyanxiananbiaozhunxiliecedingyeyicianzhaoshangshuseputiaojianjinxingceding,jilusepufengmianji,yifengmianjiweizongzuobiao,yibiaozhuncedingyedenongduweihengzuobiao,huizhibiaozhunquxian。zaijiangshiyangcedingyeanzhaoshangshuseputiaojianjinxingceding,jilusepufengmianji,genjubiaozhunquxianjisuanchushiyangcedingyezhongyanxianandenongdu。

2.8 jieguojisuan

ρ×v×s×1000

x = ——————————

真人平台m×1000×1000

shizhong:

x —yangpinzhongyanxianandehanliang,danweiweihaokemeipian(mg/pian);

真人平台ρ—congbiaozhunquxianshangchadedeyanxianandenongdu,danweiweiweikemeihaosheng(μg/ml);

真人平台v—dingrongtiji,danweiweihaosheng(ml);

真人平台s—pingjunpianzhong,danweiweike(g);

m—shiyangdechengyangliang,danweiweike(g);

1000—danweihuansuanxishu。

3 weishengsuchanliangjiance yiju《gb 5009.86》

3.1 yuanli: shiyangzhongdekanghuaixuesuanyongpianlinsuanrongjiechaoshengtiquhou,yiliziduishijiweiliudongxiang,jingfanxiangsepuzhufenli,yongpeiyouziwaijianceqideyexiangsepuyijiance。yisepufengbaoliushijiandingxing,waibiaofadingliang。

3.2 shiji

3.2.1pianlinsuan(hpo 3)n: hanliang(yihpo 3ji)≥38%。

3.2.2 linsuanerqingjia(kh 2po 4)

3.2.3shiliuwanjisanjiajixiuhuaan(c 19h 42brn): sepuchun

真人平台3.2.4jiachun(ch 3oh): sepuchun

3.2.5 biaozhunpinlaiyuanchundu: zhongjianyuan,chundu100%。

3.3yiqi

真人平台3.3.1gaoxiaoyexiangsepuyi: peiyouziwaijianceqi。

真人平台3.3.2 phji: jingdu±0.01。

真人平台3.3.3fenxitianping: ganliangwei0.1g、1mg、0.01mg。

3.3.4chaoshengboqingxiqi

真人平台3.3.5lixinji: zhuansu≥4000 r/min。

3.4 seputiaojian

a)sepuzhu: c18(zhuzhang250mm,neijing4.6mm,lijing5 μm)

b)zhuwen: 25℃

c)liudongxiang: a: 6.8glinsuanerqingjiahe0.91gshiliuwanjisanjiajixiuhuaan,yongshuirongjiebingdingrongzhi1l(yonglinsuandiaophzhi2.5~2.8);b;100%jiachun。ana: b=98: 2hunhe,guo0.45μmlvmo,chaoshengtuoqi。

真人平台d)liusu: 0.7ml/min

e)ziwaijiancebozhang: 245nm

f)jinyangliang: 20μl

3.5 biaozhunquxiandezhibei:

真人平台3.5.1 l(+)kanghuaixuesuanbiaozhunchubeirongye(1.000mg/ml): zhunquechengqubiaozhunpinl(+)kanghuaixuesuan0.01g(jingquezhi0.01mg),yong20g/ldepianlinsuanrongyedingrongzhi10ml。

1.5.2 l(+)kanghuaixuesuanbiaozhunxiliegongzuorongye: fenbiezhunquexiqul(+)kanghuaixuesuanbiaozhunrongyezhongjianye0.ml,0.05ml,0.50ml,1.0ml,2.5ml,5.0ml,yong20g/ldepianlinsuanrongyedingrongzhi100ml。biaozhunxiliegongzuorongyedefenbienongduwei0μg/ml、0.5μg/ml、5.0μg/ml、10.0μg/ml、25.00μg/ml、50.0μg/ml。

3.6 yangpinchuli

qubenpinshiliang,yanxi,jingmichengding0.5g(jingquezhi0.001g),yong20g/ldepianlinsuanrongyejiangshiyangzhuanyizhi50mlrongliangpingzhong。zhenyaorongjiebingdingrong。yaoyun,quanbuzhuanyizhi50mllixinguanzhong,chaoshengtiqu5fenzhonghou,yu4000r/minlixin5min,qushangqingyeguo0.45μmshuixianglvmo,zuoweigongshipinrongye。

真人平台3.7 yangpinceding: fenbiexiqul(+)kanghuaixuesuanbiaozhunxiliegongzuorongye10μlzhurugaoxiaoyexiangsepuyizhong,cedingxiangyingdefengmianji,yifengmianjiweizongzuobiao,yibiaozhuncedingyenongduweihengzuobiaohuizhibiaozhunquxian,jisuanhuiguifangcheng。gongshipinjinggaoxiaoyexiangsepuyifenxi,cedefengmianji,caiyongwaibiaofatongguoshangshubiaozhunquxianjisuanqinongdu。

3.8 jieguojisuan

ρ×v×s×1000

x = ——————————

真人平台m×1000×1000

shizhong:

真人平台x—yangpinzhongkanghuaixuesuandehanliang,danweiweihaokemeipian(mg/pian);

ρ —congbiaozhunquxianshangchadedekanghuaixuesuandenongdu,danweiweiweikemeihaosheng(μg/ml);

v—dingrongtiji,danweiweihaosheng(ml);

真人平台s—pingjunpianzhong,danweiweike(g);

真人平台m—shiyangdechengyangliang,danweiweike(g);

1000—danweihuansuanxishu。

【zhongliangchayizhibiao】

yingfuhe《zhonghuarenmingongheguoyaodian》zhong“zhijitongze”xiangxiapianjideguiding。

【yuanfuliaozhiliangyaoqiu】

1、rusuanxin: yingfuhegb 1903.11 《shipinanquanguojiabiaozhun shipinyingyangqianghuaji rusuanxin》deguiding

2、yanxianan: yingfuhezhongguoyaodian《yanxianan》deguiding

3、l-kanghuaixuesuan: yingfuhegb 14754 《shipinanquanguojiabiaozhun shipintianjiaji weishengsuc(kanghuaixuesuan)》deguiding

4、zhetang: yingfuhexianxing《zhonghuarenmingongheguoyaodian》deguiding

真人平台5、d-ganlutangchun: yingfuhegb 1886.177 《shipinanquanguojiabiaozhun shipintianjiaji d-ganlutangchun》deguiding

真人平台6、maiyahujing: yingfuhegb/t 20884 《maiyahujing》deguiding

7、rutang: yingfuhegb25595 《shipinanquanguojiabiaozhun rutang 》deguiding




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